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3130 a l l o y ) i n s e r t s h a v e c r a c k e d c o n siderably during the first extrusion. M o d i f i c a t i o n s o f t h e s e two m a t e r i a l s a r e being investigated i n an attempt t o f i n d a tough m a t e r i a l s u f f i c i e n t l y Exhard t o withstand t h e erosion. perience w i t h t h e mandrels is about t h e same a s w i t h t h e d i e s . The s t e e l m a n d r e l becomes s o f t , and i n t h e c a s e o f one stem 3 / 8 - i n . i n d i a m e t e r , i t actually failedintehsion.

Iodide Thorium Metal Prepared by the Van Arkel-De Boer Process. * a c o n s t a n t temperature i n a Hevi-duty p o t f u r n a c e . The t e m p e r a t u r e was cont r o l l e d a n d r e c o r d e d by m e a n s o f a Micromax c o n t r o l i ' e r w i t h a n a c c u r a c y o f f 2 O C. S i n c e r e c r y s t a l l i z a t i o n i s time-dependent, i t w a s important t o ,know t h e l e n g t h o f t i m e r e q u i r e d t o b r i n g t h e specimen t o ' t h e b a t h temp e r a t u r e .

I - I I i 1 0 47 , I C 921 ............... . ........................ . . . ......... .. 39' 1 L INTERIM REPORT ON METALLURGY OF THORIUM AND THORIUM ALLOYS .. L Transverse s e c t i o n Longi t u d i n a 1 s ec t i on - Fig. 33a Ames Thorium Extruded. C o l d - R o l l e d , Annealed 'A h r a t 7 5 0 ° C . Cycled for 1000 C y c l e s Between 100°C and 500°C io NaK. 4 . . Trans v,erse sec t i o n Longitudinal s e c t i o n - F i g . 33b Ames Thorium Extruded a t 8 5 0 ° C and C y c l e d f o r 1 0 0 0 C y c l e s Between 1 0 0 ° C - a n d SOO'C i n NaK.

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Metallurgy of Thorium, Thorium Alloys [Declassified]

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